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Formation of graphite intercalation compounds (GICs) of iron chloride in propylene carbonate PC by electrolysis was studied. Three types of structure with different interplanar distance, d 1 , were observed. The single phase of the new type having the d 1 -value of 1.03 nm (named β-type) was synthesized in dilute solution of less than 1 m. The γ-type GICs with a d 1 -value...
Electrochemical formation of graphite intercalation compounds (GICs) has been studied in the electrolyte with mixed sulfuric acid and acetic acid. The results show that, with addition of acetic acid, GICs can be synthesized in the electrolyte with sulfuric acid concentration as low as 3.6M, even though no GIC is formed in pure acetic acid. The stage structure of the synthesized GICs varies with the...
A formic acid-graphite intercalation compound (HCOOH-GIC) has been successfully synthesized by an electrochemical process whereby formic acid solution serves as both the electrolyte and the intercalate source. Stage structures of 3, 4 and 5 have been revealed by both X-ray diffraction and Raman spectroscopy. Formation of HCOOH-GIC was achieved by controlling the apparent anodic current density in...
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