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Anodised zirconium (Zr) foil at 20V for 1h in Na 2 SO 4 with 0.5wt.% NH 4 F resulted in 6μm thick anodic oxide film with nanotubular structure. At 50V the anodic layer is consisted of an irregular inner layer with the nanotubular structure only at the top of the layer. Nonetheless, the anodic oxides formed are crystalline and photocatalytic ability of the anodic oxide was assessed...
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