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High-quality porous ZnMn 2 O 4 microspheres composed of interconnected nanoparticles have been achieved by calcination of metal carbonates synthesized by a solvothermal reaction. The porous microspheres are characterized by XRD patterns, SEM, TEM, and HRTEM images to reveal the crystal phase and particle morphology. The porous structure and nanoscale building blocks of ZnMn 2 ...
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