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A novel palladium(II)‐catalyzed [5+2] oxidative annulation of readily available o‐arylanilines with alkynes has been developed for building a seven‐membered N‐heterocyclic architecture containing a biaryl linkage. This method is applicable to a wide range of unprotected o‐arylanilines and internal alkynes, and results in the chemoselective preparation of imine‐containing dibenzo[b,d]azepines in high...
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