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Au–Pd alloy octapods with the exposure of {722} facets are prepared via a seed‐mediated process at room temperature. The size of the octapods can be controlled in the range of 25–120 nm by manipulating the addition of the amount of seeds. In catalyzing the electro‐oxidation of formic acid, the as‐synthesized octapods show substantially higher activity than commercial Pd/C.
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