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The chemoselective hydrogenation from 3‐nitrostyrene to 3‐vinylaniline is quite challenging due to coexistence of the C=C bond and the –NO2 group in the same molecule. Previously, we found that the selectivity to the 3‐vinylaniline is very high in wide temperature and time windows when taking the ZnAl‐hydrotalcite supported Au25 nanoclusters as the precatalyst. Here, we investigated the loading effect...
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