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In this study, we used size-exclusion chromatography (SEC) to evaluate the sizes of Au and Au/Pd core/shell nanoparticles (NPs) that had been subjected to thermal treatment, with the eluted NPs monitored through diode array detection (DAD) of the surface plasmon (SP) absorption of the NPs. In the absence of an adequate stabilizer, thermal treatment resulted in longer retention times for the Au NPs...
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