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Polycrystalline filled skutterudite compounds Eu y Co 4 Sb 12 with 0≤y≤0.6 are synthesized by melting method and sintered by spark plasma sintering technique. The crystallographic properties are characterized by X-ray diffraction and electron probe microanalysis. The maximal filling fraction of Eu in Co 4 Sb 12 is experimentally determined to be as high as 60%,...
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