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After carefully ruling out the known sample preparation artifacts, high-angle annular detector dark-field scanning transmission electron microscopy, nanobeam composition analysis and energy-filtered imaging suggest that phase separation occurs upon heating in the Al 85 Ni 5 Y 6 Fe 2 Co 2 amorphous ribbon prior to the onset of primary crystallization, but not...
The objective of this study is to demonstrate the various artificial features introduced into metallic amorphous alloys by improper TEM sample preparation. Such artifacts are often confused with the intrinsic microstructures when examining metallic glasses under TEM. The electropolishing and ion milling procedures are compared in terms of their merits/drawbacks for avoiding/inducing artifacts in metallic...
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