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A series of layered double hydroxides (LDHs) containing Mg 2+ or Ni 2+ as divalent and Al 3+ or Ga 3+ as trivalent cations were used as catalysts in order to substitute NaOH in the selective condensation of acetone into diacetonealcohol. With this aim the LDHs were totally exchanged with OH - anions and acquired the meixnerite-like structure,...
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