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In this paper, a rimose NiZnP electrode was prepared by electroless and H2SO4 etching. This electrode acts as an efficient and stable catalytic cathode for water splitting, affording 10 mA cm−2 at an overpotential of 50 mV. It is found that using H2SO4 as an etching reagent is favorable for the formation of Ni(OH)2, and can obtain higher eletrocatalytic activity than using NaOH. It is, moreover, verified...
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