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Formaldehyde is susceptible to illegal addition to foodstuffs to extend their shelf life due to its antimicrobial, preservative and bleaching properties. In this study, a self‐supporting “nanosheet on nanosheet” arrays electrocatalyst with core‐shell heterostructure was prepared in situ by coupling NiCo layer double hydroxide with 2D ZIF derived Co‐nitrogen‐doped porous carbon on carbon cloth (Co−N/C@NiCo‐LDH...