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Analysis of the oxidation state and coordination geometry using pre‐edge analysis is attractive for heterogeneous catalysis and materials science, especially for in situ and time‐resolved studies or highly diluted systems. In the present study, focus is laid on iron‐based catalysts. First a systematic investigation of the pre‐edge region of the Fe K‐edge using staurolite, FePO4, FeO and α‐Fe2O3 as...
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