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Highly ordered, titanium-rich organically modified Ti-MCM-41 materials have been synthesized at 413 K using a mixture of organo-triethoxysilane and tetraethyl orthosilicate. Various organic substituents on Ti-MCM-41 used in the present study are methyl, vinyl, allyl, 3-chloropropyl, pentyl, and phenyl. The highest amount of Ti incorporated for a given Si/Ti mole ratio of 30 in the synthesis gel was...
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