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This article reports on a microreactor/microwave high-pressure flow hybrid apparatus of a novel concept design, which includes both the microreactor and a spiral reactor, and its efficient use in the synthesis of silver nanoparticles of relatively uniform sizes (4.3±0.7nm) under microwave irradiation. By contrast, under otherwise identical experimental conditions but with conventional heating, the...
A problem with microwave-absorbing heterogeneous catalysts (MAHCs) in non-polar solvents is resolved with a novel approach that also uses an external heating bath in combination with microwave heating. In non-polar solvents, the microwave radiation dielectrically and selectively heats only the catalyst resulting in the frequent occurrence of hot spots under these conditions. However, such hot spots...
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