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A detailed study aimed at clarifying the electrochemical behavior of Co/Al-LDH thin films, prepared on Pt electrode by electrodeposition at −0.9V, has been carried out. Reproducible thin and homogeneous films with variable amounts of LDH coated on the electrode surface have been achieved by varying the electrodeposition time (t=5, 10, 30 and 60s): 29.2±0.7, 37.9±1.4, 55.1±2.1 and 62.5±4.3μgcm ...
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