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A new photocyclization strategy by using intermolecular tandem reactions between N‐(ω‐hydroxyalkyl)‐4,5,6,7‐tetrachlorophthalimides (1, 2, and 3) and a series of acyclic and cyclic alkenes is reported. Electron transfer of the triplet‐excited phthalimide with the alkene and regioselective trapping of the alkene cation radical by the hydroxyl group at the phthalimide side chain gives a triplet 1,n‐biradical,...
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