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Three effective Ti catalysts for NaAlH 4 were made by stoichiometrically reacting TiCl 3 with LiAlH 4 in tetrahydrofuran (THF), NaAlH 4 in THF, and LiAlH 4 in diethyl ether (Et 2 O). The solid products produced after drying were named ex situ catalysts and designated respectively as Ti(Li)T, Ti(Na)T and Ti(Li)E. NaAlH 4 was dry doped with 2 mol%...
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