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A novel reduction process by spark plasma is proposed for the synthesis of homogeneous intermixed ZrB2–SiC–ZrC nanostructure powder using ZrSiO4, B2O3, C and Mg as starting materials. In the present research, the reaction mechanisms were investigated by the displacement–temperature–time (DTT), the displacement rate–temperature and the displacement rate–time diagrams which were obtained during spark...
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