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Metallic coatings in the pyrolytic graphite furnace have been used for the pre-concentration of Hg (using electrochemically reduced Au) and AsH 3 (using both thermally and electrochemically reduced Ir and Pd/Ir) prior to electrothermal volatilization. The analyte trapping efficiency during accumulation and the analyte and modifier release processes during volatilization were monitored in real...
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