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Synthesis and immobilization of caltrop cupric particles onto a Si substrate using X‐ray radiolysis directly from a liquid solution of Cu(COOCH3)2 is demonstrated. Caltrop cupric oxide particles are formed in the X‐ray radiolysis of aqueous solutions of Cu(COOCH3)2, which also contain methanol, ethanol, 2‐propanol or 1‐propanol as OH scavenger. The blade lengths of the caltrop particles are dependent...
The deposition of caltrop-shaped cupric oxide particles synthesized by X-ray radiolysis process was performed on a silicon substrate. The use of alcohol such as methanol and ethanol as an additive enabled the nucleation and growth of caltrop-shaped cupric particles, while no particles were produced in a cupric acetate solution without any alcohol with X-ray irradiation using synchrotron radiation...
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