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Precisely constructing the local configurations of active sites to achieve on‐demand catalytic functions is highly critical yet challenging. Herein, an anion‐deficient strategy to precisely capture Ru single atoms on the anion vacancies of CoP2 (Ru‐SA/Pv‐CoP2) is developed. Refined structural characterizations reveal that the Ru single atoms preferably bind to the anion vacancy sites and consequently...
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