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Reactive ball milling in hydrogen was applied to synthesize nanocrystalline Mg- and Mg8Mm20Ni-based hydrides with crystallite size below 10nm. These hydrides were studied by in situ synchrotron X-ray diffraction performed at the Swiss–Norwegian Beam Lines of the European Synchrotron Radiation Facility, Grenoble. Characterization of the phase-structural and microstructural state of the constituents...
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