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This work introduces a novel solution system not slurry to synthesize nano-micron sized Li 4 Ti 5 O 12 by spray drying followed by solid-state calcination at several temperatures between 650 and 800°C. Well-crystallized Li 4 Ti 5 O 12 with no impurity can be obtained at temperatures of 650, 700, 750 and 800 °C owing to the effect of nanoscale and uniform...
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