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To achieve a better material for thermoelectric power generation device, filled skutterudite Yb0.3Co4Sb12 samples were fabricated by melting–quenching–annealing–spark plasma sintering (SPS) method. Two sets of samples, before and after SPS, were investigated. In both the two sets of samples, the average grain size of the samples increases monotonously with the increase of annealing time, while Yb...
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