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The H2/CO2 separation properties of di/triamine vapor cross‐linked mixed matrix membranes with molecularly tuned free‐volume at 150 °C are reported. Free‐volume is molecularly tuned by altering the degree of chain‐motion using cross‐linkers with different chain lengths. A more restricted degree of chain‐motion is achieved in the cross‐linked network and the resultant membrane has a higher H2/CO2 selectivity...
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