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The electrooxidation mechanisms of guaiacol (2‐methoxyphenol), a food and beverage spoilage metabolite, and its precursors; vanillic acid (VA), vanillin, and ferulic acid (FA) were investigated by cyclic voltammetry (CV) with a boron‐doped diamond (BDD) electrode. Reversed‐phase liquid chromatography (RPLC) together with a BDD electrode poised at +1.6 V vs. Pd/H2, was optimized for their sensitive...
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