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An Fe(III)-azido complex with the formula [Fe(cyclam)(N 3 ) 2 ]ClO 4 (cyclam=1,4,8,11-tetraazacyclotetradecane) has been synthesized from the reaction of cis-[Fe(cyclam)Cl 2 ]Cl with sodium azide in methanol. The X-ray structural analysis reveals that the Fe(III) atom possesses a tetragonally compressed octahedral geometry with a trans configuration of two azido ions...
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