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The reduction of pyruvic acid in near-critical water has successfully been conducted under conditions of various temperatures, pressures, reaction time and the presence of formic acid as the reducing agent. In this work, additives (K2CO3, KHCO3, and sodium acetate) used in the reduction of pyruvic acid were also investigated. The results showed that by adding K2CO3 (25 mole %) a markedly higher lactic...
We performed the Rupe rearrangement of 1-ethynylcyclohexan-1-ol in near-critical water to study the reaction under high temperature conditions. The final product thus obtained was primarily 1-cyclohexen-1-ylethanone which was identified by GC-MS. The influences of reaction time, temperature, and initial reactant-to-water ratio on the yield of 1-cyclohexen-1-ylethanone were examined. The yield of 1-cyclohexen-1-ylethanone...
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