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Small organic molecules which can emit fluorescence with tunable dual emission bands are significant for fundamental research and broad applications. In this work, two binaphthyl based arylacrylonitrile derivatives with pyrene and triphenylamine unit (BiNp‐Py and BiNp‐TPA) were designed and synthesized, respectively, featuring chiral backbone and dual AIE‐active cyanostyrene‐linked chromophores. Excellent...
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