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Facile synthesis of hierarchically porous metal–organic frameworks (MOFs) with adjustable porosity and high crystallinity attracts great attention yet remains challenging. Herein, a micromolar amount of dye‐based modulator (Rhodamine B (RhB)) is employed to easily and controllably tailor the pore size of a Ti‐based metal–organic framework (MIL‐125‐NH2). The RhB used in this method is easily removed...
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