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The one‐pot synthesis of meso‐CF3‐substituted boron–dipyrromethene (BODIPY) compounds is achieved for the first time through the condensation of pyrroles with CF3COOH in the presence of PhSiCl3. The PhSiCl3 plays a vital role, as it provides the source of Cl– ions for the generation of acyl chloride. X‐ray crystallographic analysis revealed that the core skeleton of meso‐CF3‐BODIPY becomes nonplanar...
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