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The development of an artificial heterogeneous dyad by covalently anchoring a hydrogen‐evolving molecule catalyst to a semiconductor photosensitizer through a bridging ligand is highly challenging. Herein, we adopt the inorganic–organic hybrid CdS–DETA NSs (DETA=diethylenetriamine, NSs=nanosheets) as initial matrix to successfully construct an imine bond (‐CH=N‐) linked heterogeneous dyad [CdS−N=CH−Ni]...
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