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A plug‐flow fixed‐bed cell for synchrotron powder X‐ray diffraction (PXRD) and X‐ray absorption fine structure (XAFS) idoneous for the study of heterogeneous catalysts at high temperature, pressure and under gas flow is designed, constructed and demonstrated. The operating conditions up to 1000°C and 50 bar are ensured by a set of mass flow controllers, pressure regulators and two infra‐red lamps...
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