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A new polycyclic N-heterocyclic carbene featuring a fused dibenz[a,c]phenazine moiety was generated in situ from the corresponding tetrafluoroborate salt. The synthesis and NMR data of its corresponding precursors, its sulfur adduct and dimer are reported. Complexes of type [MCl(COD)(1)] and [MCl(CO) 2 (1)] (M = Rh and Ir, 1 = 1,3-dibutyldibenzo[a,c]phenazino[11,12-d]imidazol-2-ylidene) were...
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