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The 20 wt% Pd supported on carbon Vulcan XC-72 (Pd/C) anode catalyst, used to formic acid (FA) electro-oxidation reaction, submitted to different high temperature treatment (HTT) procedures in the temperature range 200–400 °C was studied using X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS) aided with Quantitative Analysis of Surfaces by Electron Spectroscopy (QUASES).The HTT procedures...
Samples of a palladium catalyst for direct formic acid fuel cell (DFAFC) applications were prepared on the Elat® carbon cloth by magnetron sputtering. The quantity of Pd was equal to 3.6, 120 and 720μg/cm2. The samples were tested in a fuel cell for electro-oxidation of formic acid, and were characterized by atomic force microscopy (AFM), scanning electron microscopy (SEM) and X-ray photoelectron...
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