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Novel quaternary hydrides Mg 7−x A x TiH 16−x (A=Li, Na, K) have been synthesized by use of an ultrahigh-pressure (UHP) technique. The Rietveld refinements for synchrotron X-ray diffraction (XRD) patterns suggest that added LiH and NaH greatly enhanced the yield of the Mg 7 TiH 16 phase. The unit cell volumes of the Mg 7−x A x TiH 16−x ...
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