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The new intermetallic type‐I clathrate Na8Zn4Ge42 was obtained by direct reaction of the elements, and its crystal structure was determined by means of single‐crystal X‐ray diffraction methods. The structure is described in space group Pm3n (no. 223) with a = 10.6982(1) Å. A mixed Zn/Ge occupancy is found for one of the network sites (6c). Na8Zn4Ge42 represents an air‐stable electron‐precise Zintl...
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