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WO 3 hardly dissolved in ZnCl 2 –NaCl–KCl (0.60:0.20:0.20, in mole fraction) melt at 250 °C. The solubility of WO 3 increased by the addition of KF to the melt, which enabled electrodeposition of metallic tungsten. A smooth and fine film of metallic tungsten was obtained on a nickel substrate by the potentiostatic electrolysis at 0.06 V versus Zn(II)/Zn. The thickness reached...
Molybdenum metal film has been electrodeposited in ZnCl 2 –NaCl–KCl (0.60:0.20:0.20, in mole fraction) melt containing MoCl 3 at 250°C. In this melt, a dense film was obtained by potentiostatic electrolysis at 0.15V versus Zn(II)/Zn for 3h. However, the film had a thickness of smaller than 0.5μm and was not adhesive. On the other hand, addition of 4mol% of KF to the melt led to larger...
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