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Active and highly stable oxide‐supported IrNiOx core–shell catalysts for electrochemical water splitting are presented. IrNix@IrOx nanoparticles supported on high‐surface‐area mesoporous antimony‐doped tin oxide (IrNiOx /Meso‐ATO) were synthesized from bimetallic IrNix precursor alloys (PA‐IrNix /Meso‐ATO) using electrochemical Ni leaching and concomitant Ir oxidation. Special emphasis was placed...
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