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Three mixed-ligand neutral technetium complexes containing monodentate phosphine and isothiocyanato ligands have been synthesized and studied by crystallographic methods. In the Tc(IV) compound trans-Tc(P(C 3 H 7 ) 3 ) 2 (NCS) 4 , the Tc atom is located on an inversion centre. The TcP bond distances are 2.519(3) Å while the TcN bonds are 1.991(6) and 2.003(6)...
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