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The structures of two oligomers of acidic xylo-oligosaccharides (XOS) of the same molecular weight (634 Da), Xyl2MeGlcAHex and Xyl2GlcA2 were differentiated by electrospray tandem mass spectrometry (ESI-MS/MS). These oligomers were present in a mixture of XOS obtained by acid hydrolysis of heteroxylans extracted from Eucalyptus globulus wood (Xyl2MeGlcAHex) and Olea europaea olive fruit (Xyl2GlcA2...
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