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New chiral carboranylamidophosphite ligand was synthesized and tested in the Rh-catalyzed asymmetric hydrogenation of α- and β-dehydroamino acid derivatives (up to 93% ee). The catalytic performance is affected greatly by temperature and the nature of solvents. Importantly, we have shown that in the hydrogenation of the β-dehydroamino acid derivatives the use of acidic 1,1,1,3,3,3-hexafluoro-2-propanol...
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