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Amides, such as N‐benzoylsaccharin, N,N‐diBocbenzamide, and N‐phenyl‐N‐tosylbenzamides reacted with Et3N⋅3HF to provide the corresponding acyl fluorides in good yields. The reaction was conducted under environmentally friendly conditions using i‐PrOAc as the solvent. Moreover, the reaction was performed at room temperature and did not require a transition‐metal catalyst or additives. The methodology...