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The electrochemical reactions of Li with Mn2Sb and small amounts of MnSb have been investigated by Mössbauer spectroscopy and X-ray diffraction. The lithiation transforms initially the MnSb part and later the Mn2Sb part into amorphous LiMnSb. On further lithiation the LiMnSb phase transforms to rather well crystallized Li3Sb. In the X-ray diffraction pattern for the fully lithiated sample extruded...
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