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The reactions of η 5 -Cp * M(CO) 3 Na (M = Mo, W) with α,α -p-, m- and o-dichloro-xylenes yielded p-, m- and o-xylyl bridged dinuclear complexes of η 5 -Cp * M(CO) 3 in high yields. All of such new complexes are stable to air and water, even stable in dilute acids and bases.
The reactions of R-CpMo(CO) 3 Li (R = H, Me, SiMe 3 ) with α,α'-m- and o-dichloroxylenes gave bridged dinuclear complexes of R-CpMo(CO) 3 in high yield. All of them are stable to air and water, even stable to dilute acids and bases. Complex 5 crystallizes in the monoclinic system, space group P2 1/n , with a = 12.1811(17), b = 12.0634(24), c = 17.4496(22)...
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