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The 29 Si- and 13 C-NMR spectral parameters of a range of N-(amidomethyl)-polyhalosilanes have been measured in solution and the extent of Si O bond formation and pentacoordination determined. The larger the number of electronegative groups attached to the silicon the greater the extent of pentacoordination achievable by the silicon. Thus with trichlorosilanes a 'tight'...
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