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In this work, we discuss an observed reduction of magnesium from a MgO/MgAl2O4 ceramic substrate by permeating hydrogen in thin-film Pd membranes. Membranes were fabricated via electroless plating of Pd on a porous MgO/MgAl2O4 substrate and tested under pure hydrogen permeation conditions between 500°C and 700°C. It was observed that a rapid and severe hydrogen flux decline occurred at 700°C, whereat...
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