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High surface area titania-supported materials prepared from V(IV) precursors and calcined at high temperatures have been characterized by Vis–UV diffuse reflectance, FT Raman, electron spin resonance, and X-ray photoelectron spectroscopies and tested in the partial oxidation of methane. Vanadium oxide loading and calcination temperature determine the structure of V2O5/TiO2materials. Below theoretical...
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