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Spherical rutile TiO 2 particles (14–20nm) and their corresponding well-defined round clusters (500–600nm) were obtained by using a cationic surfactant cetyltrimethylammonium bromide (CTAB). The surfactant was employed in two stages, i.e., in the hydrolysis of TiCl 4 and then in the precipitation of the corresponding Ti(IV) polymers at approximately 46°C. On the other hand, without...
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